FeCoNiMnCr high-entropy alloys (HEAs): Synthesis, structural, magnetic and nuclear radiation absorption properties

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We report the synthesis and structural, magnetic and Radiation shielding properties of High Entropy Alloy (HEA) produced through mechanical alloying method. Using an X-Ray Diffractometer (PanalyticalEmpryan) with CuK radiation at 45 kV and 40 mA, the phase identification starting elements and as-milled powders are identified. Scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDX), morphological and microstructural investigations were conducted (FEI Quanta FEG 450). EDX and elemental mapping analyses are conducted to assess the purity and elemental distributions of the synthesized alloys. Using the Quantum Design Physical Characteristics Measurement System (PPMS) with vibrating sample magnetometer (VSM) and a magnetic field of 30 kOe at room temperature, magnetic properties are examined. Using 137Cs radioisotope and mathematical methods, gamma-ray and neutron shielding properties of HEA are investigated in a conventional transmission setup using experimental and theoretical approaches. In the presence of a 3 T applied field, the sample exhibits a low magnetization of 5.30 emu/g at 300 K. Moreover, Ms is raised to 22 emu/g at 10 K owing to decreased thermal effects. The temperature dependence of the magnetization is recorded in the presence of a 1 T applied field. HEA exhibits superior neutron attenuation properties than conventional absorption materials such as B4C, graphite, and water. Our results showed that the synthesized HEA has superiority over other alloys and conventional neutron absorption materials. It can be concluded that the proposed novel HEA might be investigated further in terms of broadening its characterization and clarifying its other crucial properties to extend the scope of the current investigation.

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dc.contributor.authorŞimşek, Telem
dc.contributor.authorKavaz, Esra
dc.contributor.authorGüler, Ömer
dc.contributor.authorŞimşek, Tuncay
dc.contributor.authorAvar, Barış
dc.contributor.authorAslan, Naim
dc.contributor.authorAlmisned, Ghada
dc.contributor.authorZakaly, Hesham M.H.
dc.contributor.authorTekin, H.O.
dc.date.accessioned2026-10-28T14:54:49.587301574Z
dc.date.available2026-10-28T14:54:49.587301574Z
dc.date.issued2023
dc.description.abstractWe report the synthesis and structural, magnetic and Radiation shielding properties of High Entropy Alloy (HEA) produced through mechanical alloying method. Using an X-Ray Diffractometer (PanalyticalEmpryan) with CuK radiation at 45 kV and 40 mA, the phase identification starting elements and as-milled powders are identified. Scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDX), morphological and microstructural investigations were conducted (FEI Quanta FEG 450). EDX and elemental mapping analyses are conducted to assess the purity and elemental distributions of the synthesized alloys. Using the Quantum Design Physical Characteristics Measurement System (PPMS) with vibrating sample magnetometer (VSM) and a magnetic field of 30 kOe at room temperature, magnetic properties are examined. Using 137Cs radioisotope and mathematical methods, gamma-ray and neutron shielding properties of HEA are investigated in a conventional transmission setup using experimental and theoretical approaches. In the presence of a 3 T applied field, the sample exhibits a low magnetization of 5.30 emu/g at 300 K. Moreover, Ms is raised to 22 emu/g at 10 K owing to decreased thermal effects. The temperature dependence of the magnetization is recorded in the presence of a 1 T applied field. HEA exhibits superior neutron attenuation properties than conventional absorption materials such as B4C, graphite, and water. Our results showed that the synthesized HEA has superiority over other alloys and conventional neutron absorption materials. It can be concluded that the proposed novel HEA might be investigated further in terms of broadening its characterization and clarifying its other crucial properties to extend the scope of the current investigation.
dc.description.sponsorshipAbdulrahman University, (PNURSP2023R149)
dc.description.sponsorshipPrincess Nourah Bint Abdulrahman University, PNU
dc.identifier.doi10.1016/j.ceramint.2023.05.072
dc.identifier.eissn1873-3956
dc.identifier.endpage25370
dc.identifier.issn0272-8842
dc.identifier.issue15
dc.identifier.scopus2-s2.0-85159117727
dc.identifier.startpage25364
dc.identifier.urihttps://rdlopen.rawdatalibrary.net/r/munzur/2009
dc.identifier.volume49
dc.identifier.wosWOS:001026810500001
dc.language.isoen
dc.publisherElsevier Ltd
dc.relation.ispartofCeramics International
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectHigh entropy alloys
dc.subjectMagnetic properties
dc.subjectNuclear radiation
dc.subjectShielding materials
dc.subjectStructural properties
dc.subject.otherChromium alloys
dc.subject.otherCobalt alloys
dc.subject.otherCompressive strength
dc.subject.otherCopper alloys
dc.subject.otherEnergy dispersive spectroscopy
dc.subject.otherGamma rays
dc.subject.otherHigh-entropy alloys
dc.subject.otherIron alloys
dc.subject.otherMagnetic properties
dc.subject.otherMagnetization
dc.subject.otherManganese alloys
dc.subject.otherMechanical alloying
dc.subject.otherNeutron irradiation
dc.subject.otherNeutrons
dc.subject.otherScanning electron microscopy
dc.subject.otherStructural properties
dc.subject.otherTemperature distribution
dc.subject.otherTensile strength
dc.subject.otherWater absorption
dc.subject.otherAbsorption material
dc.subject.otherApplied field
dc.subject.otherEnergy dispersive X ray spectroscopy
dc.subject.otherHigh entropy alloys
dc.subject.otherMagnetic radiation
dc.subject.otherNuclear radiations
dc.subject.otherRadiation absorption
dc.subject.otherShielding materials
dc.subject.otherShielding properties
dc.subject.otherSynthesised
dc.subject.otherEntropy
dc.titleFeCoNiMnCr high-entropy alloys (HEAs): Synthesis, structural, magnetic and nuclear radiation absorption properties
dc.typeArticle
rdl.citation.openalex47
rdl.citation.scopus42
rdl.oa.statusgreen
rdl.oa.statusclosed
rdl.oa.urlhttps://hdl.handle.net/20.500.12628/28081
rdl.scopus.quartileQ1
rdl.source.indexSCOPUS
rdl.source.indexWOS