• MakaleYalnız künye2025Scopus SJRQ2
    Elastic modulus, nuclear radiation transmission properties of Fe-based/contained novel alloys for critical radiation applications

    ALMisned, Ghada; Susoy, Gulfem; Baykal, Duygu Sen; Alkarrani, Hessa; Güler, Ömer; Issa, Shams A.M.; Zakaly, Hesham M.H.; Tekin, H.O.

    This study explores the gamma-ray and neutron shielding properties and mechanical performance of eight Fe-based alloys with varying elemental compositions and densities. Different parameters such as mass attenuation coefficients, linear attenuation coefficients, half-value layer, tenth-value layer, mean free path, fast neutron removal cross-sections, transmission factors were analysed using PHITS and Phy-X/PSD codes. Moreover, elastic modulus values were calculated for each alloy sample. Our results reveal that the S9 alloy, with high density and tungsten contribution, exhibited superior shielding and mechanical properties, achieving the lowest TF, HVL, and TVL values. In contrast, the low-density S1 alloy performed weakest, reflecting its lighter elemental composition. Intermediate alloys like MAR-302 and Cupero-Nickel showed balanced performance, suitable for moderate shielding needs. Strong correlations between elemental compositions, particularly high-Z elements like tungsten and boron, and shielding efficiency were observed. It can be concluded that optimizing elemental composition and density is critical for designing alloys with enhanced multifunctional properties.

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  • MakaleAçık Erişim2025Scopus SJRQ1
    Examining the trade-off between structural, mechanical properties and shielding performance of Pr2O3-enhanced 316L stainless steel

    Yayla, Nihal; Albayrak, M.Gökhan; Güler, Ömer; Baykal, Duygu Sen; Alkarrani, Hessa; ALMisned, Ghada; Zakaly, Hesham M.H.; Tekin, H.O.

    This study explores the structural, mechanical, and radiation shielding properties of 316L stainless steel composites reinforced with varying weight percentages of Pr2O3. The aim is to enhance radiation attenuation capabilities while maintaining structural integrity for nuclear applications. The composites were fabricated using the mechanical alloying method, followed by detailed characterization through X-ray diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. Key radiation shielding parameters, including mass attenuation coefficient, linear attenuation coefficient, half-value layer, and effective atomic number, and transmission factor values were analysed using theoretical and computational models. Additionally, elastic modulus calculations were performed to assess mechanical properties. The results indicate that incorporating Pr2O3 significantly enhances shielding performance. The 316L-SS%20Pr2O3 composite exhibited the highest mass and linear attenuation coefficients values, with a notable reduction in half value layer values compared to the unreinforced 316L stainless steel. At lower photon energies, effective atomic number improved by 39.3 % for the 316L-SS%20Pr2O3 sample, while neutron shielding efficiency also increased. However, the elastic modulus decreased with higher Pr2O3 content, reflecting a trade-off between mechanical stiffness and radiation shielding efficiency. The findings demonstrate that 316L-SS%20Pr2O3 is a promising material for applications requiring superior radiation shielding, particularly in environments where mechanical load is secondary.

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  • MakaleAçık Erişim2023Scopus SJRQ1
    FeCoNiMnCr high-entropy alloys (HEAs): Synthesis, structural, magnetic and nuclear radiation absorption properties

    Şimşek, Telem; Kavaz, Esra; Güler, Ömer; Şimşek, Tuncay; Avar, Barış; Aslan, Naim; Almisned, Ghada; Zakaly, Hesham M.H.; Tekin, H.O.

    We report the synthesis and structural, magnetic and Radiation shielding properties of High Entropy Alloy (HEA) produced through mechanical alloying method. Using an X-Ray Diffractometer (PanalyticalEmpryan) with CuK radiation at 45 kV and 40 mA, the phase identification starting elements and as-milled powders are identified. Scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDX), morphological and microstructural investigations were conducted (FEI Quanta FEG 450). EDX and elemental mapping analyses are conducted to assess the purity and elemental distributions of the synthesized alloys. Using the Quantum Design Physical Characteristics Measurement System (PPMS) with vibrating sample magnetometer (VSM) and a magnetic field of 30 kOe at room temperature, magnetic properties are examined. Using 137Cs radioisotope and mathematical methods, gamma-ray and neutron shielding properties of HEA are investigated in a conventional transmission setup using experimental and theoretical approaches. In the presence of a 3 T applied field, the sample exhibits a low magnetization of 5.30 emu/g at 300 K. Moreover, Ms is raised to 22 emu/g at 10 K owing to decreased thermal effects. The temperature dependence of the magnetization is recorded in the presence of a 1 T applied field. HEA exhibits superior neutron attenuation properties than conventional absorption materials such as B4C, graphite, and water. Our results showed that the synthesized HEA has superiority over other alloys and conventional neutron absorption materials. It can be concluded that the proposed novel HEA might be investigated further in terms of broadening its characterization and clarifying its other crucial properties to extend the scope of the current investigation.

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  • MakaleAçık Erişim2022Scopus SJRQ2
    Synergistic effect of boron nitride and graphene nanosheets on behavioural attitudes of polyester matrix: Synthesis, experimental and Monte Carlo simulation studies

    Başgöz, Öyküm; Güler, Seval Hale; Güler, Ömer; Canbay, Canan A.; Zakaly, Hesham M.H.; Issa, Shams A.M.; ALMisned, Ghada; Tekin, H.O.

    We report the synergistic effects of boron nitride and graphene nanosheets on physical, structural, and nuclear radiation attenuation properties of polyester matrix-incorporated nanocomposites. Some critical material properties are thoroughly evaluated for several types of synthesized samples. Polyester is employed to strengthen graphene and boron nitride nanolayers, and their characteristics are investigated in detail. Additionally, we report the gamma-ray and fast neutron attenuation characteristics of synthesized nanocomposites to get a better understanding of the reinforcing effect as a function of material type and weight percentage. Thermal analysis findings indicate that adding graphene lowers the decomposition temperature but co-adding graphene and BNNS enhances thermal decomposition in comparison to graphene itself. Tensile tests showed that the inclusion of both GRP and GRP/BNNS strengthens the material. Among the polyester composite samples analyzed, the G3 sample with the most GNP reinforcement had the lowest HVL values throughout the broadest range of energy levels investigated. The recent findings may be beneficial to the scientific community in terms of incorporating these reinforcing types and ratios into polyester materials for a variety of applications, including industrial and research purposes.

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  • MakaleAçık Erişim2022Scopus SJRQ1
    Synthesis and structural, electrical, optical, and gamma-ray attenuation properties of ZnO-multi-walled carbon nanotubes (MWCNT) composite separately incorporated with CdO, TiO2, and Fe2O3

    Basgoz, Oykum; Guler, Omer; Evin, Ertan; Yavuz, Cagdas; ALMisned, Ghada; Issa, Shams A.M.; Zakaly, Hesham M.H.; Tekin, H.O.

    In this study, Fe2O3, TiO2, and CdO semiconductor metal oxides were separately incorporated into the ZnO-MWCNT composite at different weight percentages. Accordingly, several experimental analyses on electrical, optical, and radiation shielding characteristics of coupled semiconductor metal oxides nanocomposites were performed to determine their monotonic impact on the investigated material properties. Moreover, gamma-ray shielding properties of these novel materials were determined using MCNPX general-purpose Monte Carlo code. At 5% oxide addition, the maximum electrical conductivity was found in all groups for all temperatures. Moreover, 5% oxide reinforcement resulted in the maximum reflection characteristics in all groups. Among the CdO doped materials, the CZnOCd5 sample exhibits the highest electrical conductivity behaviour at room and high temperatures. The Eg value calculated for the CZnOCd5 sample was 3.284 eV. The CZnOCd2.5 and CZnOCd5 samples had the greatest Eg values when compared to the pure sample and the samples from other groups. The CZnOCd5 sample has the highest reflectance value in the CZnOCd group's reflectance graph. On the other hand, the maximum gamma-ray attenuation properties were reported for CZnOCd5 sample. Among the analysed samples, the CZnOCd5 sample's characteristics provide a preliminary motivation for a more comprehensive analysis of this material and assessment of potential radiation protection applications.

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