Sürdürülebilir Kalkınma Amaçları

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• MakaleYalnız künye2022Scopus SJRQ3/r/munzur/2952
  Boron-incorporated biocomposite coatings on 316L and NiTi alloys: Enhanced structural, antibacterial activity, and cell viability performances

  Aslan, N.; Aksakal, B.; Aksoy, M.E.

  Boron doped (5 %, 10%, and 15 wt.%) Hydroxyapatite (B-HA) biocomposites were syntesized and coated on 316L SS and NiTi (Ni-45Ti) metallic substrates by using the electrophoretic deposition process (EPD). The morphological and structural characterization of the coatings was executed using scanning electron microscopy (SEM) and X-ray diffraction devices (XRD). Antibacterial tests were conducted using Escherichia coli (E. coli, JM103) and Staphylococcus aureus (S. aureus, ATCC29293) microorganisms. The mitochondrial activity assay (MTT)-[3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide] was used to examine cell viability and cytotoxicity in Saos-2 osteoblast cells. HA and boron peaks, as well as B-TCP and metallic components, were detected in XRD examinations. Porous morphologies were generated on the surface with boron doped B-HA coatings, as revealed by SEM views. Antibacterial activity studies revealed that both metallic coating groups, notably with boron doping, demonstrated antibacterial activity against gram-negative E. coli and gram-positive S. aureus. The antibacterial activity of the 316L group was shown to be better than that of the NiTi group in comparisonal testing. The syntesized boron-doped biocomposite coatings did not have any detrimental effects on living cells, according to cell viability studies. The cell viability rate was found to be greater in NiTi coatings than in 316 SS coatings, and the impact was amplified by the addition of boron.

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  AtıfScopus6·WoS4·OpenAlex7

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• DüzeltmeAçık Erişim2022Scopus SJRQ2/r/munzur/2625
  Correction to: Boron-Doped Hydroxyapatite Coatings on NiTi Alloys Using the Electrophoretic Deposition Method: Enhanced Corrosion and Adhesion Performances (Journal of Materials Engineering and Performance, (2021), 30, 10, (7365-7375), 10.1007/s11665-021-05968-x)

  Aksoy, M.E.; Aksakal, B.; Aslan, N.; Dikici, B.

  The following acknowledgment was inadvertently omitted from the originally published article: This work was supported by Yildiz Technical University, C¸ AP (Grant No. FCD-2019-3511).

  AtıfScopus1·WoS1·OpenAlex1

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• MakaleYalnız künye2021Scopus SJRQ3/r/munzur/2585
  Enhanced Adhesion and Corrosion Properties of Boron Doped Bioceramic Coated 316L Implants

  Aksoy, M.E.; Aksakal, B.; Aslan, N.; Dikici, B.

  Abstract: In order to provide an effective prevention to 316L implants, a synthesized bioceramic was coated by using electrophoretic deposition (EPD). The effect of boron addition into hydroxyapatite (HA) on surface morphology, adhesion and corrosion resistance of the implant has been examined. Boron doped HA (B–HA) was synthesized by a simple chemical acid-base method with 5, 10, and 15 wt % boron additions to coat on 316L implants. The synthesized B-HA was coated on the substrates and the coated surfaces with and without B additions. Sintering took place at different temperatures and sintering rates. The coatings were characterized by X-ray diffractometer (XRD), Fourier transform infrared spectroscopy (FT–IR) and scanning electron microscope (SEM). Furthermore, adhesion and in vitro corrosion tests were conducted. The influence of boron additons on adhesion and corrosion resistance of 316L have been revealed for the coated substrates at different B additions. It was shown that boron addition increased the adhesion and corrosion resistance of the bioceramic coatings. Furthermore, the sintering effect on adhesion was also evaluated and the highest adhesion as 25.8 MPa has been reached at 750°C for 90 s and 5°C min–1 sintering conditions. It was found that using iodine as EPD dispersant has increased the charging ability of the B–HA powders in the suspension and hence eased deposition rate. The study revealed that boron-containing hydroxyapatite coatings can provide crack-free surfaces that providing high adhesion and hence increase the corrosion resistance of metallic implants. Through the results, it was also shown that the network between powders was improved and hence adhesion was increased with increasing B addition.

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  AtıfScopus10·WoS9·OpenAlex12

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• MakaleYalnız künye2021Scopus SJRQ2/r/munzur/2511
  Boron-Doped Hydroxyapatite Coatings on NiTi Alloys Using the Electrophoretic Deposition Method: Enhanced Corrosion and Adhesion Performances

  Aksoy, M.E.; Aksakal, B.; Aslan, N.; Dikici, B.

  Metallic implants are functionalized with coatings due to the need to protect against biological corrosion in the body. Hydroxyapatite (HAp) has desirable biocompatibility and structural properties, but poor mechanical properties limit its use as a standalone coating. In this study, boron-doped hydroxyapatite (B-HAp) biocomposites containing 5, 10, and 15% boron by weight were synthesized by the sol-gel method and applied as a coating to NiTi using electrophoretic deposition (EPD). The deposition was carried out for 60, 90, and 120 s, and sintering at 750 °C for 75 minutes under vacuum. The coated substrates were then characterized by XRD, SEM, and FT-IR, and their adhesion strengths and in-vitro corrosion behaviors in simulated body fluid were compared with uncoated samples. The results showed that the microporous powders formed well-bonded structures, which positively affect adhesion strength. The highest adhesion strength (30 MPa) and corrosion resistance were achieved with 15 wt.% B-HAP coating at 120 s deposition time and 76.5 μm coating thickness.

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  AtıfScopus18·WoS16·OpenAlex19

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