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Yayınlar
- MakaleYalnız künye2019Scopus SJRQ2Modelling cadmium bioaccumulation in Gammarus pulex by using experimental design approach
Serdar, Osman; Pala, Aysegul; Ince, Muharrem; Onal, Ali
Recently, although dynamic approaches have been used increasingly to describe metal bioaccumulation in aquatic organisms, the validation of such laboratory-derived modelling is rarely assessed under environmental conditions. The present study aims to evaluate and verify statistical and mathematical models for the bioaccumulation of cadmium (Cd) and to evaluate the suitability of Gammarus pulex as a biomonitor for Cd. To optimise Cd2+ ion bioaccumulation conditions a Box–Behnken design was used and whether G. pulex can be used as an estimated tool to assess aquatic quality was investigated. A Box–Behnken experimental design combined with response surface modelling (RSM) was employed for Cd2+ bioaccumulation in G. pulex. Independent variables including temperature, contact time and Cd2+ ion concentration significance and their interactions were tested using analysis of variance. The selected variables’ optimum values were obtained by solving the quadratic regression model along with by analysing the response surface contour plots. Based on Box–Behnken design, the applied model is significant because model F-value and R2 were obtained as 5121.49, 0.9998, respectively. Bioaccumulation of Cd amount was analysed using electrothermal atomic absorption spectrophotometer. The obtained data suggest that G. pulex can be evaluated as Cd biomonitor.
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İncele - MakaleAçık Erişim2019Scopus SJRQ4Modeling approach with Box-Behnken design for optimization of Pb bioaccumulation parameters in Gammarus pulex (L., 1758)
Pala, Aysegul; Serdar, Osman; Ince, Muharrem; Onal, Ali
The aim of this research was to evaluate the suitability of Gammarus pulex (L., 1758), an amphipod crustacean, as a bio-monitor for lead (Pb). A Box– Behnken experimental approach combined with response surface modeling (RSM) and quadratic programming was employed to increase the knowledge about Pb2+ bioaccumulation in Gammarus pulex (L., 1758). Independent variables, such as temperature ranging from 18 to 22 ºC, contact time from 8 to 48 hours, and Pb2+ ion solution concentrations from 50 to 100 µg L-1, were studied and tested using analysis of variance (ANOVA). The standardized effects of the independent variables and their interactions on the dependent variable were also investigated according to a Pareto chart. The selected variables' optimum values were obtained by solving the quadratic regression model along with analyzing the response surface contour plots. Optimum experimental conditions were obtained at 22.0 ºC, contact time of 8 hours, and Pb concentration at 69.5 µg L-1. Based on the Box-Behnken design, the applied model is significant because the model F-value and R2 were obtained at 77.80 and 0.9901, respectively. Bioaccumulation of Pb was determined using electrothermal atomic absorption spectrometry (ETAAS). The obtained data suggest that G. pulex can be used as a Pb biomonitor.
AtıfScopus4WoS6OpenAlex6İncele - MakaleAçık Erişim2019Scopus SJRQ2Using Box–Behnken design approach to investigate benzo[a]anthracene formation in smoked cattle meat samples and its’ risk assessment
Kaplan Ince, Olcay; Ince, Muharrem
In present study, a novel approach was selected for benzo[a]anthracene determination from smoked cattle meat samples using solid phase extraction under various experimental conditions. To optimize experimental variables, a three factor, three-level Box–Behnken experimental design combining with response surface methodology and quadratic programming were employed to prevent excessive amount of benzo[a]anthracene formation in smoked meat based on different experimental parameters. The influence of some important process parameters including cooking time (10–30 min), fat ratio (5–25%) and distance to the cooking source (5–25 cm), which significantly affected the formation efficiency of benzo[a]anthracene were optimized. The analysis of variance was conducted for specifying the interactions of independent variables. The independent and the dependent variables interactions were investigated. The quadratic regression model and the response surface contour plots were used to determine optimum values for the selected variables. The results of study revealed that optimum cooking time of smoked cattle meat was determined as 24.9 min, fat ratio 7.9% and the distance to the cooking source 21.8 cm. Under optimum conditions, minimum benzo[a]anthracene was formed in meat and its amount was determined using high performance liquid chromatography-mass spectrophotometer as qualitative and quantitative. The limit of detection and limit of quantitation values were calculated as 0.4 µg kg −1 and 1.1 µg kg −1 , respectively.
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İncele - MakaleYalnız künye2019Scopus SJRQ3Determination of antioxidant capacity using different acidified solvents and element contents of Allium tuncelianum: A regional and varietal study on endemic edible garlic
Karaaslan, Nagihan M.; Ince, Muharrem; Kaplan Ince, Olcay; Goksin Karaaslan, Merve
Allium tuncelianum (Tunceli garlic), an endemic and threatened plant species in the Tunceli province of Eastern Turkey, is an important native source for local people. The antioxidant activities of the acidified extracts of water, acetonitrile, methanol, and ethanol of Allium tuncelianum were investigated using five antioxidant capacity tests. The results indicated that methanol extract efficiencies of garlic samples using the ABTS, CUPRAC, and reducing power capacities were higher than the other extracts. Water extract and acetonitrile extract values were highest for total phenolic content and metal chelating activities, respectively. Moreover, the element contents such as calcium (Ca), copper (Cu), iron (Fe), potassium (K), magnesium (Mg), manganese (Mn), sodium (Na), and zinc (Zn) of Allium tuncelianum samples digested by microwave and ashing ovens were determined by flame atomic absorption spectrophotometry and the results were compared statistically. The Ca, Cu, K, Mg, and Zn concentrations using the microwave method were found to be higher than the ashing procedure. However, the Fe, Mn, and Na concentrations using the ashing method were found to be higher than those using the the microwave protocol.
AtıfScopus7WoS6OpenAlex7İncele - MakaleYalnız künye2018Scopus SJRQ3Response surface modeling for Pb(II) removal from alcoholic beverages using natural clay: Process optimization with box–behnken experimental design and determination by electrothermal AAS
Ince, Olcay Kaplan; Ince, Muharrem; Onal, Ali
A three-level four-factor Box–Behnken experimental design (BBD) combined with response surface modeling (RSM) was used for the optimization and modeling of Pb(II) adsorption from alcoholic beverages onto natural clay. The BBD method was chosen as the statistical prediction method to reduce the experimental numbers which saves time and chemicals and reduce analysis cost. Various independent process variables including solution pH (X1: 3.0– 7.0), contact time (X2: 2–60 min), adsorbent dosage (X3: 0.01-0.1 g), and agitation speed (X4: 50–150 rpm) were optimized. The optimal conditions used for Pb(II) removal were pH of 5.3, contact time 38.9 minutes, 0.071 g adsorbent dosage, and 98.7 rpm agitation speed, resulting in a maximum removal efficiency of 120 mg g-1. Pb was determined by electrothermal AAS. The significance of the independent variables and their interactions were tested by means of the analysis of variance (ANOVA) and are based on the ANOVA statistical value. The adsorption of Pb(II) onto clay was found to be highly significant with very low probability (p) values (<0.001). These results were justified by the relatively high correlation coefficients (R2 = 0.9965, R2 adj = 0.9930, and R2 Pred= 0.9819) of the statistical prediction. FTIR analysis confirmed major participation of amide, amines, ketones, including the primary alcohol groups, during Pb(II) biosorption. Clay was characterized by Fourier transform infrared spectroscopy (FTIR) and scanning electron microscope (SEM), coupled with energy dispersive X-Ray (EDX). The proposed adsorption process efficiently removes Pb(II) present in various aqueous media and can be used for industrial wastewater or drinks.
AtıfScopus6İncele - MakaleYalnız künye2017Scopus SJRQ1A food waste utilization study for removing lead(II) from drinks
Ince, Olcay Kaplan; Ince, Muharrem; Yonten, Vahap; Goksu, Ali
This is the first study about removal of lead (Pb(II)) from energy drinks. In this paper, food waste, namely eggshell (hydroxyapatite) utilization, was used to remove Pb(II) from mineral water and energy drinks. Mineral water and energy drinks were chosen for removal of lead since the latter is severely hazardous to human health even in small amounts. Response Surface Methodology (RSM) was performed to optimize the application process by practice of the quadratic model united with the Central Composite Design (CCD) and quadratic combined program was utilized to study the most effective parameters on aforementioned liquids. Through the application of variance analysis (ANOVA) factors critical to removing of lead were identified for each experimental design response. Maximum adsorption capacity of eggshell was achieved as 923 mg g(-1) for Pb(II). The obtained optimum conditions were applied to drinks. Results showed that used adsorbent was quite effective in removing Pb(II) from drinks. (C) 2016 Elsevier Ltd. All rights reserved.
AtıfWoS27OpenAlex28İncele - DüzeltmeYalnız künye2017Scopus SJRQ1A food waste utilization study for removing lead(II) from drinks (vol 214, pg 637, 2017)
Ince, Olcay Kaplan; Ince, Muharrem; Yonten, Vahap; Goksu, Ali
- MakaleYalnız künye2017Scopus SJRQ3Box-Behnken design approach for optimizing removal of copper from wastewater using a novel and green adsorbent
Ince, Muharrem; Ince, Olcay Kaplan
The aim of the present research was to apply the Box-Behnken experimental design and response surface methodology for modeling of copper (Cu2+) ions from an industrial wastewater and leachate pretreated astragalus herbal plant. A three factor, three level Box-Behnken experimental design combined with response surface modeling (RSM) and quadratic programming (QP) was employed for maximizing Cu(ID removal from aqueous solution based on 17 different experimental data obtained in a batch experimental study. Three independent variables (pH ranging from 2.0 to 8.0, contact time from 10 to 180 minutes, and adsorbent amount from 0.1 to 1 g) were studied. The significance of the independent variables and their interactions were tested by means of the analysis of variance (ANOVA) with 95% confidence limits. The standardized effects of the independent variables and their interactions on the dependent variable were also investigated by preparing a Pareto chart. The optimum values of the selected variables were obtained by solving the quadratic regression model as well as by analyzing the response surface contour plots. Using the experimental conditions of pH = 5.0, contact time = 92.5 minutes, adsorbent dosage = 0.25 g, the recovery efficiency of Cu(II) was found to be 100%. Copper-free and copperloaded astragalus was analyzed using fourier transform infrared spectrometry (FTIR) which evidenced the functional groups involved in copper uptake. Adsorption equilibrium for copper was described by using the Freundlich and Langmiur adsorption isotherms. This adsorbent was applied to different industrial wastewater and leachate samples for copper removal.
AtıfScopus17İncele - BildiriYalnız künye2017Removal of copper from aqueous solution using perlite
Tanaydin, Mehmet Kayra; Tanaydin, Zümra Bakici; Ince, Muharrem; Demlrkiran, Nizamettin; Akdemir, A.O.; Ekinci, A.; Han, I.; Oztekin, A.; Set, E.; Dadasoglu, F.
The wastewaters containing organic and inorganic pollutants after many industrial processes such as metal plating, mining, textile, alloy, battery and industrial chemicals, are often discharged to environment. Heavy metals among these pollutants have highly stable, toxic, non-degradable and carcinogenic characters. They affect not only ecological system, but also human health and many life forms. Therefore, these contaminants should be eliminated or reduced to allowable levels before releasing to environment. Most of heavy metals have toxic character even at low concentrations of about 0.1-0.3ppm. Treatment technologies such as filtration, ion exchange, precipitation, electrodeposition, reverse osmosis, sedimentation, and adsorption have been applied for removal of heavy metals from aqueous solutions. Adsorption is one of the most common and widely applied methods to eliminate the metal ions from waste solutions because of its simplicity and cost effectiveness. Activated carbon, clay minerals, ion exchange resins and various agricultural residues can be used as adsorbent materials in this process [1-3].
AtıfScopus1WoS1OpenAlex3İncele - MakaleAçık Erişim2017Scopus SJRQ2Optimization of an Analytical Method for Determination of Pyrene in Smoked Meat Products
Ince, Muharrem; Kaplan Ince, Olcay; Yaman, Mehmet
In the present study, an analytical method was optimized for determination of pyrene by solid-phase extraction in Turkish foodstuffs including chicken and grilled meat samples. In accordance with this purpose, all of the parameters that may affect the signal of pyrene during analysis processes were optimized using high-performance liquid chromatography–mass spectrometry system. The optimized parameters for column temperature, injection volume, mobile-phase flow rate, and fragmentor potential were found to be 45 °C, 60 μL, 0.6 mL min−1, and 130 V, respectively. The optimized high-performance liquid chromatography–mass spectrometry method was applied for the determination and evaluation of pyrene in food samples that include chicken and grilled meat. The pyrene amount in meat samples was obtained in the range from 2.3 to 4.4 μg kg−1 for the normal grilled meat and chicken samples and from 12 to 135 μg kg−1 for exceedingly grilled samples. The results show that the concentration of pyrene is significantly dependent on the type of meat sample and cooking source. The limit of detection and quantitation was found to be 0.5 μg L−1 and 1.53 μg L−1, respectively.
AtıfScopus5WoS5OpenAlex7İncele - MakaleYalnız künye2017Scopus SJRQ3Using food waste biomass as effective adsorbents in water and wastewater treatment for Cu(II) removal
Ince, Muharrem; Ince, Olcay Kaplan; Asam, Eren; Önal, Ali
The present study investigated Cu(II) ion adsorption onto banana peel, chestnut shell, and tea leaf waste in aqueous medium under different experimental conditions. Batch adsorption studies were carried out with various Cu(II) concentrations as well as the influence of process parameters such as pH, contact time, and adsorbent amount on the removal of copper, and the optimum conditions for maximum removal of copper from an aqueous solution. These food waste biomass adsorbents were applied to mineral water and industrial wastewater samples and the copper removal potentials were compared. The nature of the adsorbents and metal ion interactions was examined by the fourier transform infrared spectroscopy (FTIR) technique. The adsorption data were obtained by using the Langmuir model showing maximum adsorption capacity of banana peel, chestnut shell, and tea leaf waste at 1.94 mg g-1 2.25 mg g-1, and 3.36 mg g-1, respectively. Copper was determined by flame atomic absorption spectrometry.
AtıfScopus19İncele - MakaleAçık Erişim2016Scopus SJRQ2Optimization of Remazol Brilliant Blue R dye removal by novel biosorbent P. eryngii immobilized on Amberlite XAD-4 using response surface methodology
Yonten, Vahap; Tanyol, Mehtap; Yildirim, Numan; Yildirim, Nuran Cikcikoglu; Ince, Muharrem
This study investigates preparation of biosorbent Pleurotus eryngii immobilized on Amberlite XAD-4 and the optimal conditions for removal of Remazol Brilliant Blue R (RBBR) reactive dye from synthetic aqueous solutions. The process was optimized using the response surface methodology (RSM) developed by the application of the quadratic model associated with the central composite design. For this purpose, RSM was employed to determine the effects of operational parameters on this material as effective and available adsorbent. The investigated variables were dye initial concentration (10-60 mg L-1), solution pH (2-9), adsorbent dosage (0.1-0.5 g), and temperature (20-45 degrees C). The significant factors on each experimental design response were identified from the analysis of variance (ANOVA). The RSM indicated that optimum conditions of initial dye concentration, pH, adsorbent dosage, and temperature for maximum RBBR removal (98%) were achieved as 36.3 mg L-1, 2.0, 0.304 g, and 38.7 degrees C, respectively. The results showed that this biosorbent was an appropriate adsorbent for the removal of RBBR from aqueous solutions.
AtıfWoS17OpenAlex20İncele - MakaleYalnız künye2016Scopus SJRQ3Optimization of Cadmium Removal from Water by Hydroxyapatite Using Experimental Design Methodology
Ince, Olcay Kaplan; Ince, Muharrem; Karaaslan, Nagihan M.; Yonten, Vahap
The presence of cadmium in water is a serious threat to the environment. The removal of cadmium using hydroxyapatite as an adsorbent was studied in an aqueous system. Hydroxyapatite was prepared to process the adsorption of cadmium from aqueous solution. Experimental design methodology and response surface methodology (RSM) with a quadratic model associated with central composite design was used to optimize the pH, initial heavy metal concentration, final volume, and adsorbent dosage for the removal of cadmium. Analysis of variance identified significant factors on each parameter. RSM indicated that a pH of 8.5, a sample volume of 166 mL, an adsorbent of dosage 0.57 g, and a contact time of 82 min were optimal for the adsorption of Cd(II). Under these conditions, the removal of Cd(II) was 895 mg g(-1).
AtıfWoS17OpenAlex15İncele - MakaleAçık Erişim2016Scopus SJRQ2Nickel, Lead, and Cadmium Removal Using a Low-Cost Adsorbent - Banana Peel
Ince, Muharrem; Ince, Olcay Kaplan; Yonten, Vahap; Karaaslan, Nagihan M.
Water pollution because of inorganic contaminants is a serious problem due to the acute toxicities and carcinogenic nature of pollutants. Recently, much attention has been focused on using natural and low-cost adsorbents, especially food residues, for removing toxic metal ions. Batch removal of nickel (Ni(II)), lead (Pb(II)), and cadmium (Cd(II)) from aqueous solution using a natural adsorbent is described in this study. Effects of various parameters on adsorption capacities such as pH, adsorbent dose, and stirring time were investigated by batch experiments. The maximum adsorption capacities for Ni(II), Pb(II), and Cd(II) ions were 1.6 mg g(-1), 125 mg g(-1), and 84 mg g(-1), respectively. Characterization of the surface modification was performed with FTIR measurements. FTIR spectra showed that chemisorption takes place at the surface of the adsorbent. The Freundlich and Langmuir adsorption isotherms were used to evaluate the equilibrium data. The characteristic parameters for each isotherm were determined. The Langmuir and Freundlich isotherm provided the best correlation for Ni(II), Cd(II), and Pb(II) using banana peel.
AtıfWoS10OpenAlex13İncele - MakaleAçık Erişim2016Scopus SJRQ2Adsorption of bisphenol A from aqueous solutions by Pleurotus eryngii immobilized on Amberlite XAD-4 using as a new adsorbent
Yonten, Vahap; Ince, Muharrem; Tanyol, Mehtap; Yildirim, Numan
The adsorption of bisphenol A (BPA) in a fixed-bed column was evaluated in this work. Fungus Pleurotus eryngii isolated from Tunceli (Turkey) immobilized on XAD-4 resin was used as an adsorbent for decontamination of BPA from aqueous solutions. The extent of BPA removal capacity was evaluated as a function of parameters such as pH, volume of the sample, and column bed height. Adsorption isotherms of BPA on immobilized P. eryngii were determined and correlated with common isotherm equations such as Langmuir and Freundlich models. The mechanism of adsorption of BPA was analyzed preadsorption (XAD-4+fungus) and postadsorption (XAD-4+fungus+BPA) using fourier transform infrared spectroscopy. The results show that adsorption ability of BPA by immobilized P. eryngii is possible and this system yields the best degree of BPA removal (90%) at pH 11 for an initial load of 120mgL(-1). Therefore, this material can be used as a very effective adsorbent for BPA decontamination in aqueous solutions.
AtıfWoS17OpenAlex21İncele - MakaleAçık Erişim2014Scopus SJRQ3Comparision of Low-Cost and Eco-Friendly Adsorbent for Adsorption of Ni(II)
Ince, Muharrem
In this study, samples of clay, tea waste, astragalus plant, chestnut shell, and egg shell were used as low-cost and eco-friendly adsorbents for the adsorption of Ni(ID from aqueous solutions. The effect of various parameters such as pH, contact time, adsorbent dose, and final volume on the adsorption capacities of these natural adsorbents were investigated by batch experiments. The adsorption capacity for Ni(II) was found to be 19.4 mg g(-1), 5.4 mg g(-1) 1.3 mg g(-1), 5.6 mg g(-1), 72.0 mg g(-1) for clay, tea waste, astragalus plant, chestnut shell, and egg shell, respectively. Egg shell has maximum adsorption capacity at pH 12, 45-minute contact time, and 0.5 g adsorbent mass. Nickel-free and nickel-loaded adsorbents were characterized by FTIR spectroscopy, which evidenced the functional groups involved in nickel uptake. This work investigated the utilization of eco-friendly and low-cost adsorbents as an alternative natural adsorbent for Ni(II) ions.
AtıfWoS18OpenAlex14İncele - MakaleYalnız künye2013Scopus SJRQ3FLAME ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF NICKEL AND CHROMIUM IN VARIOUS PLANT LEAVES USED AS BIOMONITORS IN ENVIRONMENTAL POLLUTION
Avci, Halim; Kaya, Gokce; Akdeniz, Ismail; Ince, Muharrem; Yaman, Mehmet
Levels of nickel and chromium in leaves of 14 plant species grown in industrial sites of Gaziantep and surrounding were examined for biomonitoring of atmospheric pollution using flame atomic absorption spectrophotometry (FAAS). The plant leaf samples were collected from different locations with different degrees of metal pollution. The metal levels in the plants were in the ranges of (with mean values) 0.4-28.0 (3.1) mg kg(-1) for Ni and 0.1-6.6 (1.5) mg kg(-1) for Cr. On the other hand, the Ni and Cr levels in the plant leaf samples collected from control) areas were in the ranges of 0.4-2.1 (1.1) and 0.1-1.4 (0.58) mg kg(-1), respectively. It was concluded that Pinus nigra L., Acacia robinia L., Platanus orientalis L., Nerium oleander L., Pyracantha coccinea M.Roem. and Populus nigra L. for Ni, Pinus nigra L., Acacia robinia L., Olea europaea L. and Nerium oleander L. for Cr could be biomonitors. Therefore, it was demonstrated that the plant leaves could be used for heavy metal air pollution monitoring in urban and industrial regions.
AtıfWoS10İncele - MakaleYalnız künye2012Scopus SJRQ4High Performance Liquid Chromatography-Mass Spectrometry for Determination of Benzo[a]pyrene in Grilled Meat Foods
Ince, Muharrem; Yaman, Mehmet
The concentrations and varieties of benzo[a]pyrene were determined in Turkish foodstuffs including grilled meat and chicken samples by high performance liquid chromatography-mass spectrometry (HPLC-MS). The parameters that are thought to affect the response in the HPLC-MS analysis were optimized. The optimized conditions were found to be 0.75 mL min(-1) for flow rate of mobile phase, 45 mu L for injection volume, 55 degrees C for column temperature and 140 V for fragmentor potential. The optimized method was applied for the determination of benzo[a]pyrene concentrations in grilled meat and chicken foods. The obtained concentrations were found in the range of 2.7-8.3 mu g kg(-1) for the normal grilled meat and chicken samples and 72-138 mu g kg(-1) for over-grilled samples. The results showed that the concentrations of benzo[a]pyrene were significantly dependent on the kind of meat and the cooking time and source. The limits of detection and quantitation were found to be 0.7 and 2.33 mu g L-1, respectively.
AtıfWoS1İncele - MakaleAçık Erişim2011Scopus SJRQ4Determination of Elements in Thermal Springs for Monitoring Pre-Earthquake Activites by ICP-MS
Yaman, Mehmet; Sasmaz, Ahmet; Kaya, Gokce; Ince, Muharrem; Karaaslan, Nagihan M.; Ozcan, Cemile; Akkus, Sukran
AtıfOpenAlex3İncele - MakaleAçık Erişim2011Scopus SJRQ2Sequential extraction of cadmium in different soil phases and plant parts from a former industrialized area
Kaplan, Olcay; Ince, Muharrem; Yaman, Mehmet
Cd concentrations in mobile phases of soil are more representative than total Cd concentration for estimating Cd bioavailability, physicochemical reactivity and mobility. In this study, selective sequential extraction procedures were used to determine Cd in different soil phases. Soil samples and plants grown in these soils were collected from a serpentine and copper-mining area in Maden-Elazig-Turkey. The extracted fractions were exchangeable/carbonate, reducible-iron/manganese oxides, oxidizable-organic matter and sulfides, and residual phases except silicates. Concentrations of Cd in soils and plant samples were determined by flame atomic absorption spectrometry and inductively coupled plasma-mass spectrometry. We found that Cd concentrations in the EDTA and NH(2)OH center dot HCl extracts are higher in most soil samples compared to the other extracts. We conclude that Cd levels in mobile phases are unexpectedly high. The observed Cd concentrations are in ranges of 0.03-3.4 mg kg(-1) for soil and 0.02-2.5 mg kg(-1) for plant parts. The percentages of cadmium up to 56% in exchangeable and carbonates fractions were observed to be significantly higher than in those values less than 2% reported in literature. This study has shown that the modified extraction method can be usefully applied to determine Cd concentrations in potentially mobile phase of soil. Furthermore, it was concluded that Brassicasea and Rumex leaves can be used as hyperaccumulator plants because their translocation factor and/or enrichment coefficient values were found to be higher than 1.0.
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