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  • MakaleAçık Erişim2024Scopus SJRQ1
    Design of Ohmic Thawing Cell with Hydrostatic Pressure Units: Application in Minced Beef

    Döner, Deniz; Çokgezme, Ömer Faruk; Çevik, Mutlu; İçier, Filiz

    The thawing process is a common processing method used in the meat industry. To ensure provide food safety and protect meat quality, the thawing process should be carried out carefully. Ohmic thawing (OT) is one of the novel thawing methods. In this study, a custom-designed ohmic thawing prototype was set up and used to thaw frozen minced beef samples in different shapes (X: 13 × 4 × 3 cm3; Y: 13 × 6 × 2 cm3; Z: 13 cm height × 3.91 cm diameter) at 3 different voltage gradients (10–13-16 V/cm) by using 3 different electrode designs (E1, titanium foil; E2, needle type titanium electrode; E3, titanium embossed). The optimum OT condition resulting in a high-quality product with the highest process efficiency was determined. As an optimization procedure, a three-level general factorial design was performed. Thawing time, drip loss, thawing ratio, maximum temperature, ohmic power consumption, energy efficiency, and exergy efficiency values were used as responses. The cylindrical sample shape resulted in higher changes in quality and decreased performance of the process. The optimum ohmic thawing condition was a 16 V/cm voltage gradient for Y-shaped samples by using an E2 electrode design. The thawing time for the optimum condition was 2074s corresponding ohmic power consumption of 15.84 W. The drip loss during thawing was measured at 1.20%. The maximum temperature reached during the thawing process was recorded as 15.90 °C. Energy efficiency and exergy efficiency values were greater than 35%. Based on these results, the overall desirability of the ohmic thawing method was evaluated as 0.755. The obtained desirability value indicated the ohmic thawing method to be highly efficient and effective in achieving optimal thawing outcomes. The results of this study could give valuable information on the design of industrial-scale ohmic heating units to be used with solid foods, especially for thawing purposes.

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  • MakaleYayıncıda açık erişim2024Scopus SJRQ1
    Investigation of in-vitro bioactivity, electrochemical corrosion, wettability and adhesion properties of bioglass-based coatings modified with Y2O3 and Zr on novel β-type Ti-30Zr-5Mo alloys

    Dikici, B.; Say, Y.; Zhao, X.; Niinomi, M.; Szechyńska-Hebda, M.

    In this study, the in-vitro bioactivity, electrochemical corrosion resistance, wettability, and adhesion properties of bioglass-based coatings modified with Y2O3 and ZrO2 on Ti-30Zr-5Mo alloy were investigated. The coatings were prepared using the sol-gel method and applied to the alloy substrates through dip-coating. The surface morphology and elemental composition of the coatings were analyzed using SEM/EDS and XRD techniques. Potentiodynamic polarization (PDS) and electrochemical impedance spectroscopy (EIS) were employed to assess the electrochemical behavior of the coatings under in-vitro conditions. Contact angle measurements were conducted to evaluate the wettability of the surfaces. Adhesion strength was measured using tensile testing in accordance with ISO 13779-2 standards. Bioactivity tests were performed by immersing the samples in simulated body fluid (SBF). The results demonstrate that the addition of Y2O3 and ZrO2 improves adhesion strength and corrosion potential, but introducing localized galvanic effects that increase the corrosion current density. Besides, the coatings maintained their structural integrity after the bioactivity tests, and promoted new apatite formation.

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  • MakaleYalnız künye2024Scopus SJRQ1
    Effect of Zr content on microstructure and wear behavior of Al-Si-Cu-Ni Mg-Zrx alloy

    Taşgın, Yahya; Gök, Mehmet

    In this study, the effect of zirconium addition (1, 1.5, 2 wt%) on the microstructural morphology and wear behavior of Al-Si-Cu-Ni-Mg alloys, known as light metals in which intermediate phases solidify rapidly at high temperatures, was investigated. The study aimed to obtain a stronger material by modifying the Al81Si12Cu4Ni2Mg alloy. It was observed that the Zr added to the alloy was homogeneously distributed throughout the samples. Aluminum and silicon formed compounds with zirconium (Al3Zr and ZrSi2), leading to the formation of a thinner and stronger structure. With the heat treatment applied to the aluminum alloys, the structure became more ductile. Additionally, as a result of Zr addition, microhardness increased, and wear values improved. Graphical abstract: (Figure presented.)

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  • MakaleAçık Erişim2024Scopus SJRQ2
    Innovative Al6061-gadolinium oxide ods alloys: fabrication and comprehensive characterization of microstructural, physical, mechanical, and radiation shielding properties

    ALMisned, Ghada; Yayla, Nihal; Albayrak, M. Gökhan; Güler, Ömer; Baykal, Duygu Sen; Tekin, H.O.

    This study explores the development and comprehensive characterization of Al6061-Gd₂O₃ composites, designed to enhance radiation shielding and mechanical properties for critical applications in environments exposed to ionizing radiation. The purpose of this research is to assess the effectiveness of Gd2O3 as a reinforcing material for Al6061, with the aim of creating a dual-function composite that combines structural integrity with superior gamma-ray and neutron attenuation capabilities. Using X-ray diffraction (XRD) and scanning electron microscopy (SEM), we analyzed the microstructural effects of varying Gd2O3 content, observing homogeneous dispersion at low concentrations and clustering at higher levels. Mechanical properties demonstrated that increased Gd2O3 content reduces the elastic modulus, indicating a trade-off between stiffness and shielding efficiency. Radiation shielding parameters, including Transmission Factor (TF), mass attenuation coefficient (MAC), and Fast Neutron Removal Cross Section (FNRCS), were evaluated through Phy-X/PSD and PHITS Monte Carlo simulations. Results indicate that Gd2O3 reinforcement significantly improves gamma-ray and neutron shielding, particularly at higher concentrations, making the composite viable for non-structural applications prioritizing radiation protection. The findings from this study highlight the potential of Gd2O3-reinforced Al6061 composites to serve as effective shielding materials in environments where radiation exposure is a primary concern.

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  • MakaleAçık Erişim2024Scopus SJRQ2
    Photocatalytic Hydrogen Evolution of TiZrNbHfTaOx High-Entropy Oxide Synthesized by Mechano-Thermal Method

    Güler, Ömer; Boyrazlı, Mustafa; Albayrak, Muhammet Gökhan; Güler, Seval Hale; Ishihara, Tatsumi; Edalati, Kaveh

    One of the most promising solutions to slow down CO2 emissions is the use of photocatalysis to produce hydrogen as a clean fuel. However, the efficiency of the photocatalysts is not at the desired level, and they usually need precious metal co-catalysts for reactions. In this study, to achieve efficient photocatalytic hydrogen production, a high-entropy oxide was synthesized by a mechano-thermal method. The synthesized high-entropy oxide had a bandgap of 2.45 eV, which coincided with both UV and visible light regions. The material could successfully produce hydrogen from water under light, but the main difference to conventional photocatalysts was that the photocatalysis proceeded without a co-catalyst addition. Hydrogen production increased with increasing time, and at the end of the 3 h period, 134.76 µmol/m2 h of hydrogen was produced. These findings not only introduce a new method for producing high-entropy photocatalysts but also confirm the high potential of high-entropy photocatalysts for hydrogen production without the need for precious metal co-catalysts.

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  • MakaleAçık Erişim2024Scopus SJRQ2
    Enhanced impedance, electrical conductivity, dielectric properties for colloidal starch-g-poly (methyl methacrylate) supported with semiconductor cadmium sulfide

    Torğut, Gülben; Gürler, Nedim

    In this study, starch-graft-poly (methyl methacrylate) (starch-g-PMMA) composites doped with different amounts (5, 10, and 15 wt%) of cadmium sulfide (CdS) particles were fabricated for electrical measurements using in-situ polymerization technique. The structural characterization of the samples was studied. The dielectric and conductivity properties of the composites were investigated using impedance analyzer depending on the frequency (100 Hz–20 kHz) at room temperature. Spectroscopy revealed that the dielectric constant (ε′), dielectric loss (ε′′), and real (Z) components of impedance are found to decrease with increasing frequency for both starch-g-PMMA and starch-g-PMMA (5, 10, and 15 wt%) composites. On the contrary, the AC conductivity (σac) of samples increased with increasing frequency. In addition, ε′ and ε′′ values of starch-g-PMMA were lower than composites that added CdS. When the CdS content increased from 0 to 15%, ε′ increased from 5.62 to 15.10 at 100 Hz. AC conductivity was improved after adding the CdS particles. The maximum conductivity value for starch-g-PMMA15%CdS is found to be 3.07 × 10–7 at 100 Hz. When the dielectric properties of composites are evaluated, it is concluded that it is an exciting material for electronic applications in technology.

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  • MakaleYayıncıda açık erişim2024Scopus SJRQ1
    Effect of pretreatment temperature and time on fat bonding and fat reduction in deep-fried surimi

    Erol, Nida Demirtas; Cakli, Sukran; Szymczak, Mariusz; Shen, Cangliang; Matak, Kristen E.; Jaczynski, Jacek

    Deep frying (DF) is a popular cooking technique resulting in desirable sensory quality. However, DF also results in negative perception related to increased fat uptake and thus poor nutritional quality. In this study, a development of a novel strategy for fat reduction in DF surimi without additives and coatings was attempted. Novel pre-baking and pre-roasting were applied to surimi prior to DF. This novel pre-treatment strategy for DF surimi has not been reported in literature. Total, free, and bonded fat contents and corresponding fat reductions in DF surimi were determined. Cook and moisture losses as well as water holding capacity, expressible moisture, in addition to color and texture were also investigated. Fat uptake during DF of surimi was reduced (P < 0.05) by ≥ 25 % with pre-baking. Pre-baking improved (P < 0.05) or did not (P > 0.05) affect cook and moisture losses, water holding capacity, expressible moisture, color, and texture. However, pre-roasting increased (P < 0.05) fat content and adversely affected most quality parameters. Pre-baking of surimi at lower-temperature (116 °C) for longer-time (12–15 min) followed by DF at lower-temperature (170 °C) for longer-time (4 min) was most optimal for fat reduction, cook and moisture losses, water holding capacity, expressible moisture, color, and texture of surimi.

    • SDG 2 · Açlığa Son
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  • MakaleAçık Erişim2024Scopus SJRQ1
    Integrated Approach Using Intuitionistic Fuzzy Multicriteria Decision-Making to Support Classifier Selection for Technology Adoption in Patients with Parkinson Disease: Algorithm Development and Validation

    Ortiz-Barrios, Miguel; Cleland, Ian; Donnelly, Mark; Gul, Muhammet; Yucesan, Melih; Jiménez-Delgado, Genett Isabel; Nugent, Chris; Madrid-Sierra, Stephany

    Background: Parkinson disease (PD) is reported to be among the most prevalent neurodegenerative diseases globally, presenting ongoing challenges and increasing burden on health care systems. In an effort to support patients with PD, their carers, and the wider health care sector to manage this incurable condition, the focus has begun to shift away from traditional treatments. One of the most contemporary treatments includes prescribing assistive technologies (ATs), which are viewed as a way to promote independent living and deliver remote care. However, the uptake of these ATs is varied, with some users not ready or willing to accept all forms of AT and others only willing to adopt low-technology solutions. Consequently, to manage both the demands on resources and the efficiency with which ATs are deployed, new approaches are needed to automatically assess or predict a user’s likelihood to accept and adopt a particular AT before it is prescribed. Classification algorithms can be used to automatically consider the range of factors impacting AT adoption likelihood, thereby potentially supporting more effective AT allocation. From a computational perspective, different classification algorithms and selection criteria offer various opportunities and challenges to address this need. Objective: This paper presents a novel hybrid multicriteria decision-making approach to support classifier selection in technology adoption processes involving patients with PD. Methods: First, the intuitionistic fuzzy analytic hierarchy process (IF-AHP) was implemented to calculate the relative priorities of criteria and subcriteria considering experts’ knowledge and uncertainty. Second, the intuitionistic fuzzy decision-making trial and evaluation laboratory (IF-DEMATEL) was applied to evaluate the cause-effect relationships among criteria/subcriteria. Finally, the combined compromise solution (CoCoSo) was used to rank the candidate classifiers based on their capability to model the technology adoption. Results: We conducted a study involving a mobile smartphone solution to validate the proposed methodology. Structure (F5) was identified as the factor with the highest relative priority (overall weight=0.214), while adaptability (F4) (D-R=1.234) was found to be the most influencing aspect when selecting classifiers for technology adoption in patients with PD. In this case, the most appropriate algorithm for supporting technology adoption in patients with PD was the A3 - J48 decision tree (M3=2.5592). The results obtained by comparing the CoCoSo method in the proposed approach with 2 alternative methods; (simple additive weighting and technique for order of preference by similarity to ideal solution) support the accuracy and applicability of the proposed methodology. It was observed that the final scores of the algorithms in each method were highly correlated (Pearson correlation coefficient >0.8). Conclusions: The IF-AHP-IF-DEMATEL-CoCoSo approach helped to identify classification algorithms that do not just discriminate between good and bad adopters of assistive technologies within the Parkinson population but also consider technology-specific features like design, quality, and compatibility that make these classifiers easily implementable by clinicians in the health care system.

    • SDG 3 · Sağlık ve Kaliteli Yaşam
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  • MakaleYalnız künye2024Scopus SJRQ4
    A Note on a New Bivariate Copula Defined with a Piecewise Generator Function

    Chesneau, Christophe; Susam, Selim Orhun

    Copulas are essential probability tools for characterizing the joint distribution of random variables. In this article, we contribute to the topic by studying special bivariate copulas. They have the property of being defined with piecewise components and are designed for the analysis of data that have dependence structures with distinct substructures in square zones. The theoretical properties of the copulas are studied, with emphasis on their mathematical validity and some dependence measures. In particular, it is shown that the Kendall tau coefficient has a simple expression that is governed by several parameters, demonstrating the flexibility of the approach. In addition, a real data example is provided to demonstrate the applicability of the copulas. Fair comparisons with other standard copulas motivate their use in other practical scenarios.

  • MakaleYalnız künye2024Scopus SJRQ2
    Effects of Cr and W in TiMoNb Refractory High Entropy Alloys

    Simsek, Tuncay; Kurtulus, Altug; Avar, Baris; Güler, Seval Hale; Dag, İlker Emin; Chattopadhyay, Arun K.

    This study focuses on synthesizing and characterizing mechanically alloyed refractory high entropy alloys (RHEA) containing TiMoNb, Cr, W, and Cr + W. Analytical techniques including XRD, SEM, EDX, DTA, and TGA were employed to explore the influence of Cr and W on the alloys' structure, morphology, and thermal stability towards oxidation. XRD analysis confirmed the formation of a single-phase bcc solid solution in TiMoNbCr, TiMoNbW, and TiMoNbCrW alloys. Crystallite size decreased as milling progressed, yielding average sizes of approximately 7.2 nm, 7.4 nm, and 9.7 nm, with lattice strains of 1.143%, 1.148%, and 1.15%, respectively. Both experimental and calculated values of lattice parameters converged to around 3.1685 ± 0.002 and 3.1791 ± 0.010 Å for all three alloys. The synergy of Cr and W in TiMoNb was observed for the first time, impacting dislocation density, hardness, and oxidation stability. TiMoNbCrW exhibited reduced dislocation density and the highest hardness (502 HV). TGA indicated enhanced oxidation resistance up to 400 °C for TiMoNbCrW compared to the most vulnerable TiMoNbCr alloy.

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  • MakaleAçık Erişim2024Scopus SJRQ1
    Changes in quality characteristics and inactivation of Salmonella in cake, including oleogel used as a fat replacer, baked with two different methods

    Ozdemir-Orhan, Necla; Eroglu, Zeynep; Omac, Basri

    This is the first study to assess the impact of substitution of shortening (50%) with sunflower-beeswax oleogel in cake formulations on the inactivation kinetics of Salmonella spp. and the quality attributes of cakes baked in conventional (CO) and microwave (MWO) ovens. Four distinct cake samples were examined in the study: Cake samples containing oleogel prepared in two different ovens (Oleo-Cake-CO and Oleo-Cake-MWO) and control cake samples baked in two different ovens (Cont-Cake-CO and Cont-Cake-MWO). The control-batter and oleogel-batter demonstrated shear thinning behavior (pseudoplastic, n < 1), with a good fit to the Power Law model, but viscosity and viscoelastic moduli decreased when the oleogel was used in place of shortening in cake recipes. In addition, the Cont-Cake-MWO had the greatest special volume value (2.31 ± 0.04 mL/g), whereas the Oleo-Cake-CO had the lowest (1.65 ± 0.02 mL/g) (p < 0.05). Furthermore, compared to the samples baked with CO, lower water activity and moisture values (p < 0.05) were observed in the samples baked in MWO due to their higher cooking loss values (p < 0.05). In all baking techniques, the addition of oleogel to the cake formula, used as a fat substitute, resulted in higher values for cohesiveness, hardness, springiness, and chewiness (p < 0.05). As a result, the inactivation of Salmonella in cakes slightly reduced with using oleogel as a fat substitute (p > 0.05), whereas it affected some quality properties of cakes baked with both heat treatments.

    • SDG 2 · Açlığa Son
    • SDG 3 · Sağlık ve Kaliteli Yaşam
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  • MakaleAçık Erişim2024Scopus SJRQ4
    Perceived COVID-19 anxiety, fear and depression levels among university students during the decreased restrictions of COVID-19 pandemic

    Baş, Kazım

    Introduction and aim. The COVID-19 pandemic has negatively impacted human life. It is observed that a significant group affected by this situation are university students. Evaluating the psychological states of students during the transition to normal life from the pandemic period is important. This study was conducted to examine the perceived levels of COVID-19 anxiety, fear, and depression among university students during the descreased restrictions of the COVID-19 pandemic. Material and methods. This cross-sectional study was conducted with 1170 university students. The data were collected using “the Introductory Information Form, the Fear of COVID-19 Scale, the Coronavirus Anxiety Scale – Short Form, and the Depression Scale. Results. It was observed that there was a difference between gender, class, education level, income level, having had COVID-19, and having a deceased relative due to COVID-19 and perceived COVID-19 anxiety and fear and depression levels among university students (p<0.05). Conclusion. During the COVID-19 pandemic, although restrictions have been lifted, students still experience moderate levels of COVID-19 anxiety, fear, and depression. Therefore, considering the factors that affect university students’ mental state, there is a need for services that support students’ mental well-being.

    • SDG 3 · Sağlık ve Kaliteli Yaşam
  • MakaleAçık Erişim2024Scopus SJRQ3
    Four bryophyte species new to Türkiye and South-West Asia

    Batan, Nevzat; Taşçi, Nurtaç; Mamontov, Yuriy S.; Erata, Hüseyin; Alataş, Mevlüt; Ezer, Tülay

    Scapania praetervisa, Scapania mucronata, Solenostoma confertissimum, and Platyhypnum alpinum found as new to Türkiye following a recent bryofloristic excursion in Artvin region (Caucasian part of Türkiye). Platyhypnum alpinum is also new to Asia. Descriptions, illustrations, distributions, habitat characteristics, and comparisons with morphologically similar taxa are briefly given.

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  • MakaleAçık Erişim2024Scopus SJRQ2
    The influence of cold rolling and hydroxyapatite coating on the mechanostructure, corrosion resistance, cell viability, and antibacterial activity of ZnCu biodegradable implants

    Aksakal, B.; Karadogan, S.A.; Aslan, N.; Fidan, F.; Yilmazer, Y.; Sezek, S.

    Zinc (Zn) and its alloys exhibit great potential for utilization in biodegradable bone implants. Zn-1Cu biodegradable alloy was produced and were cold rolled at two different deformation rates of 47 and 61%. The samples have been bioceramic coated with the sol–gel method and microstructure-mechanical property changes, corrosion behavior and biocompatibility of the samples were investigated. They were characterized by Optical, SEM, XRD and wettability analysis. The rolled samples showed a significant increase in hardness when compared to the non-rolled samples. The unrolled and 47% rolled samples showed better corrosion resistance compared to 61% rolled samples. Antibacterial effects of the base and sol–gel-coated groups showed higher cell viability ratios than the uncoated groups. Cell viability increased significantly in 47% of the rolled samples after 24, 48, and 72 h, however decreased by up to 70% in 61% of the rolled samples. Graphical abstract: (Figure presented.).

    • SDG 3 · Sağlık ve Kaliteli Yaşam
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  • MakaleYalnız künye2024Scopus SJRQ2
    Evaluating the metallographic properties and performance of heat transfer by natural convection of graphene-coated glass used for heating

    Kahraman, Gökhan; Taşgın, Yahya

    In this study, a decorative electric heater was manufactured to reduce carbon emissions related to residential and office heating, and this heater was metallographically evaluated. In addition, the heating performance of the manufactured plate was investigated by examining its heat transfer capacity by natural convection. For this purpose, the surface of the tempered glass plate was coated with graphene by spraying to improve its electrical and heat conduction properties. Copper strips were attached to both sides of the plate to allow for an electric current. The plate was connected to mains electricity, and its change in surface temperature over time was measured. Using the measured temperature values, the heat transfer rate by natural convection on the plate surface was calculated. As a result of the calculations, it was determined that the graphene-coated tempered glass plate reached a heating performance of 40 watts after 2400 s of electrical energy supply. This value can be increased by increasing the heat transfer surface area. This study, taking advantage of the excellent thermophysical properties of graphene, will contribute to other studies conducted in this field.

    • SDG 7 · Erişilebilir ve Temiz Enerji
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  • MakaleYalnız künye2024Scopus SJRQ1
    Ks estimates using macroscopic capillary length estimated from soil hydraulic shape coefficients and Haverkamp infiltration model

    Yilmaz, Deniz; Sağlam, Mustafa; İç, Serkan; Stewart, Ryan D.; Lassabatere, Laurent

    In this study, we developed a new general approach to estimate the macroscopic capillary length (λc) using different hydraulic function models and related shape parameters, along with the Haverkamp infiltration model constant. We next applied this new approach to the van Genuchten model coupled with a Burdine condition (vGB) to estimate λc. Then, we applied the new λc computation to three different methods for estimating saturated hydraulic conductivity (Ks), and analyzed two sets of constant infiltration data: 1) an analytically generated Beerkan-type dataset and 2) constant head and Beerkan-type infiltration tests performed at the Ambarköprü Experimental Station of Blacksea Agricultural Research Institute in Samsun, Turkey. Our new approach provided accurate Ks estimates when applied to the analytical Beerkan infiltration data. The highest error was observed for a silt soil, with 30 % error for one formulation versus <15 % for the others. For synthetic coarse-textured soils such loamy sand and sandy loam, the error was <10 %. For the field data and Beerkan-type experiments, the new approach gave consistent estimates of Ks regardless of analytical interpretation. However, ANOVA analysis revealed that Ks varied between different infiltration test types, with constant head infiltrometry with 5 cm of applied water head having greater Ks values than the Beerkan tests (p < 0.05). Estimated Ks values also differed between land use types (p < 0.01), with a maize field having significantly greater Ks compared to a soybean field. Overall, we conclude that the proposed approach represents an efficient and appropriate method for characterizing point-scale saturated hydraulic conductivity, so long as experimental artifacts such as ring insertion deep and preferential flows are considered.

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  • MakaleYalnız künye2024Scopus SJRQ2
    Synthesis and characterization of MgO-doped PHA bio-composites

    Aydın, Handan

    In this study, a highly useable MgO doped polymer composite of Polyhydroxyalkanoates (PHA), which is an alternative to conventional plastics and an environmentally friendly plastic material due to its biodegradability, was investigated. PHA-MgO composites were obtained by stirring in a suitable solution for a long time with the help of a homogenizer. Then, MgO was added and the changes in Poly Hydroxy Alkonate (PHA) polymer composites were investigated according to the changing MgO ratio. Composites were prepared by adding MgO at different ratios of 1 %, 5 %, 10 % and 15 % into PHA. The structural results of the prepared samples were investigated by using XRD (X-Ray Diffraction) and SEM (Scanning Electron Microscopy). In addition, the thermal properties of the composites were investigated by DSC (Differential Scanning Calorimetry) and TGA (Thermogravimetric Analysis). Furthermore, the optical properties of PHA-MgO composites were determined by UV-VIS spectrometry. Finally, since PHA polymer exhibits shape memory properties, the shape memory properties of the composites were also investigated.

    • SDG 12 · Sorumlu Üretim ve Tüketim
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  • DüzeltmeAçık Erişim2024Scopus SJRQ2
    Correction: Genotoxic effects of copper nanoparticles on Vicia pannonica Crantz. root meristem cells (Journal of Nanoparticle Research, (2024), 26, 8, (185), 10.1007/s11051-024-06096-y)

    Tasar, Neslihan

    The original version of this article unfortunately contained incorrect Figs. 2, 3, and 4. Lastly, Open access cancellation shall be initiated. The approval manager initially approved the article by mistake, and they approved it above their maximum article threshold by accident. (Figure presented.) (Figure presented.) (Figure presented.) A Adhesion in prophase, B distorted prophase, C metaphase, D distorted metaphase, E non-collection in metaphase plaque, F lagging chromosome in metaphase, G adhesion in metaphase, H chromosome loss in metaphase, I chromosome breakage in metaphase, J asynchronous division in anaphase, K distorted anaphase, L lagging chromosome in anaphase, M polar deviation in anaphase, N chromosome bridges in anaphase, O advance in anaphase, P polar deviation in telophase, R bridge in telophase, S lagging chromosome in telophase, T distorted telophase, U adhesion in telophase (magnification = × 100) A The scanning electron microscopy (SEM) image of the control group, EDS characteristic spectrum, and mapping image. B The scanning electron microscopy (SEM) image of the sample that was prepared with 50 ppm Cu NPs, EDS characteristic spectrum, and mapping image. C The scanning electron microscopy (SEM) image of the sample that was prepared with 150 ppm Cu NPs, EDS characteristic spectrum, and mapping image. D The scanning electron microscopy (SEM) image of the sample that was prepared with 300 ppm Cu NPs, EDS characteristic spectrum, and mapping image The XRD plots of the samples that were obtained from V. pannonica plant grown with Cu (40–60 nm) NP

  • MakaleAçık Erişim2024Scopus SJRQ3
    Synthesis and characterization of chitosan-based pH-sensitive biofilm: An experimental design approach for release of vitamin B12

    Onal, Ali; Demir, Hulya; Ince, Olcay Kaplan; Ince, Muharrem

    Hydrogels because of their unique potentials, such as highwater content and hydrophilicity, are of interest for the controlled release of drug molecules. In the present study, a biofilm was produced using chitosan, a natural polymer. Characterization analyses of the synthesized biofilm were performed using Fourier-transform infrared spectroscopy (FT-IR), thermogravimetric analysis-differential thermal analysis, x-ray diffraction, and scanning electron microscopy-energy dispersive x-ray spectrometry. The analysis results of the film before loading were compared to the analysis made after adding vitamin B12 to the film. The release percentage of vitamin B12 was investigated by using ultraviolet-visible spectrophotometery. The FT-IR bands of vitamin B12 were in the range of 2,800-3,500 cm-1 and 1,000 cm-1-1,750 cm-1. When pH increased from 3 to 7, release of vitamin B12 from the biopolymer increased up to pH 5. While examining the release potential, parameters, such as pH, initial concentration of vitamin B12, release time, and solution volume, were optimized by using response surface methodology. It was determined that with the increase in release time and the initial concentration, pH contributed positively to the release of vitamin B12. The following conditions were determined for release of vitamin B12 from the biofilm: pH: 4.2, initial concentration of vitamin B12: 54.0 mg L-1, the release time: 117 min, and volume of solution: 2.1 mL. The analysis of variance results showed that the determination coefficients for the use of synthesized biofilm in vitamin B12 release were high and R2 =0.9704.

    • SDG 3 · Sağlık ve Kaliteli Yaşam
    AtıfScopus9WoS9OpenAlex10
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  • MakaleAçık Erişim2024Scopus SJRQ1
    Determining the Levels of Cortisol, Testosterone, Lactic Acid and Anaerobic Performance in Athletes Using Various Forms of Coffee

    Gür, Melda; Çınar, Vedat; Akbulut, Taner; Bozbay, Kenan; Yücedal, Polat; Aslan, Mehdi; Avcu, Gökçe; Padulo, Johnny; Russo, Luca; Rog, Joanna

    Background: Coffee is considered one of the most preferred and consumed beverage types in the world, and caffeine is known to increase physical performance due to its ergogenic properties. The aim of this study is to examine the effects of coffee consumption in different forms on cortisol, testosterone, lactic acid and anaerobic performance levels. Methods: A total of 15 licensed male football players participated in the research voluntarily. The research was implemented in a single-blind, counterbalanced, randomized and crossover study design. Participants were given caffeinated coffee (CK), decaffeinated coffee (placebo) (DK), powdered caffeine (in a gelatin capsule) (PC) and powdered placebo (maltodextrin in a capsule) (PM) on different days, and the Wingate test protocol was performed after the warm-up protocol. Blood samples were collected post-test. Cortisol, testosterone and lactic acid levels in the serum samples taken were determined by the ELISA method. Results: As a result, it was revealed that caffeinated coffee given to participants who exercise increased anaerobic power. However, it was observed that lactic acid levels were higher in placebo and decaffeinated coffee. The highest level of cortisol was found in caffeinated coffee and powdered caffeine compared to the placebo. Testosterone values were observed to be highest in caffeinated coffee and decaffeinated coffee compared to a placebo. Conclusions: The study suggests that the type of caffeine is a factor that affects absorption rate, which impacts performance and hormone levels.

    • SDG 3 · Sağlık ve Kaliteli Yaşam
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