Sürdürülebilir Kalkınma Amaçları
Yazarlar
- Aksakal, B.(7)
- Say, Y.(4)
- Aksakal, Bunyamin(3)
- Aslan, N.(3)
- Say, Yakup(3)
- Aksoy, M.E.(2)
- Dikici, B.(2)
- Alak, Gonca(1)
- Aslan, Naim(1)
- Aydoğdu, Burcu(1)
- Aytar, Mehmet(1)
- Bakirdere, S.(1)
- Buyukpinar, Ç.(1)
- Demirel, Mehtap(1)
- Dikici, Burak(1)
- Fidan, Ferzan(1)
- Ince, Muharrem(1)
- Ince, Olcay Kaplan(1)
- Karaaslan, Nagihan M.(1)
- Koç, Mümin Mehmet(1)
- Kuzgun, Nermin Karaton(1)
- Nakai, M.(1)
- Niinomi, M.(1)
- Sinirlioglu, Zeynep A.(1)
- Topuz, M.(1)
- Unal, Ilkay(1)
- Unal, İlkay(1)
- Yilmazer, H.(1)
- Yonten, Vahap(1)
Yayınlar
- MakaleYalnız künye2025Scopus SJRQ2Hydrocolloid materials of fish bone-derived in edible films: can hydroxyapatite be an alternative approach to improving fillet shelf life?
Alak, Gonca; Kuzgun, Nermin Karaton
The valorization of industrial fish waste has gained significant scientific interest due to its integrated benefits such as waste management and resource recovery. The aim of this study is to evaluate the effectiveness of fish bones, which is one of the wastes of aquaculture processing and constitutes approximately 9–15% of the waste generated as a result of the process, as a preservative in the food industry within the scope of green chemistry applications, sustainability and green product targets. In line with this objective, in the first stage, hydroxyapatite (HAP) was obtained from the fish bones, in the second stage, chitosan (Ch)-based coating solutions were enriched with HAP at different levels (0.02, 0.04 and 0.08 g / L) and in the last stage, fillets were coated with this solution and fillet quality parameters were monitored by microbiological, chemical and sensory analyses at certain intervals (0, 3, 6, 9 and 12 days) during 12 days of storage (at + 4 °C). Based on the data obtained during the storage period, the shelf life of control (Chitosan, Ch). chitosan + low HAP (Ch + L-HAP) and chitosan + medium HAP (Ch + M-HAP) fillet groups increased by 50%, 26% and 20%, respectively, compared to chitosan + high HAP (Ch + H-HAP). In the findings obtained, it was determined that the high concentration application (Ch + H-HAP) had a negative effect on all the parameters studied in fillets, and when the data on the last day of storage, especially the microbiological results were taken into consideration, it was determined that the shelf life decreased by 20–50% on average compared to the other concentrations (Ch + L-HAP and Ch + M-HAP) and Ch group and caused serious negativities in sensory parameters. Based on this result, it would be useful to try low and medium levels of this compound in different combinations. These findings indicate that HAP-enriched chitosan coatings have potential as a promising delivery system for the effective and controlled transport of bioactive ingredients in the food industry.
AtıfScopus5WoS5OpenAlex5
İncele - MakaleAçık Erişim2025Scopus SJRQ1Green Synthesis of Multi-Walled Carbon Nanotube-Reinforced Hydroxyapatite Doped with Silver and Silver-Core Selenium-Shell Nanoparticles: Synthesis, Characterization, and Biological Activity
Unal, İlkay
Hydroxyapatite (HAp) is widely used in biomedical applications due to its biocompatibility, osteoconductivity, and bioactivity. However, its low mechanical strength, tendency toward rapid corrosion, and lack of bactericidal properties present significant limitations in applications. This study aimed to improve the properties of HAp by reinforcing it with multi-walled carbon nanotubes (MWCNTs) and doping it with silver nanoparticles (AgNPs) and silver-core selenium-shell nanoparticles (Ag@SeNPs). Ocimum basilicum extract was used as both a reducing and stabilizing agent in the synthesis of nanoparticles using an environmentally friendly and non-toxic method as an alternative to traditional methods. The synthesized HAp, HAp/MWCNT, Ag-HAp/MWCNT, and Ag@Se-HAp/MWCNT nanocomposites were characterized by TEM, SEM, XRD, Raman spectroscopy, and BET analysis. BET analysis showed a reduction in surface area from 109.4 m2/g for pure HAp to 71.4 m2/g, 47.5 m2/g, and 35.3 m2/g for HAp/MWCNTs, Ag- HAp/MWCNTs, and Ag@Se-HAp/MWCNTs, respectively. Antimicrobial activities against P. aeruginosa, E. coli, S. aureus, E. faecalis, and C. albicans were evaluated. HAp and HAp/MWCNT did not show any antimicrobial activity, while Ag-HAp/MWCNTs showed inhibition zones of 14 mm for Escherichia coli and 18 mm for Pseudomonas aeruginosa at 5 mg/mL. Ag@Se-MWCNTs/HAp exhibited superior efficacy with inhibition zones of 18 mm, 12 mm, and 20 mm for S. aureus, E. faecalis, and Candida albicans, respectively. The incorporation of Ag@SeNPs enhanced HAp’s antibacterial and antifungal properties through a synergistic mechanism.
AtıfScopus12WoS10OpenAlex12
İncele - MakaleYalnız künye2024Scopus SJRQ2Synthesis and characterization of TiNbZrMo medium-entropy bio-composites: Microstructure, mechanical properties, and in vitro degradation
Say, Yakup
This study reports the synthesis and characterization of hydroxyapatite (HA)-based bio-composites reinforced with varying amounts (by weight, 1–15 wt.%) of bio-medium entropy alloy (BioMEA) for load-bearing implant applications. BioMEA powders consisting of Ti, Nb, Zr, and Mo were mechanically alloyed for 100 h and subsequently added to HA using powder metallurgy techniques. To show the effect of BioMEA, the microstructure, density, and mechanical tests have been conducted and the synthesized BioMEA was characterized by scanning electron microscope (SEM), x-ray diffractometer (XRD), and Fourier-transform infrared spectroscopy (FTIR) analysis. In addition, in vitro degradation behavior and bioactivity analyses of bio-composites have been conducted. XRD analysis revealed the formation of BioMEA after 20 h of mechanical alloying. The highest density value of 2.47 g/cm3 was found in 15 wt.% BioMEA-reinforced bio-composite. The addition of BioMEA reinforcement led to a significant increase in hardness and tensile strength values, with the highest values observed at 15 wt.% reinforcement. Compression tests demonstrated a significant increase in compressive strength and deformation capability of the bio-composites with the highest values observed at 15 wt.% BioMEA addition. The highest toughness of 7.68 kJ/m2 was measured in 10 wt.% MEA-reinforced bio-composites. The produced bio-composite materials have an elastic modulus between 3.5–5.5 GPa, which may provide a solution to the stress shielding problems caused by the high elastic modulus of metallic implant materials. The most severe degradation occurred in 15 wt.% MEA-reinforced bio-composites, and the effect of degradation caused a decrease in Ca and an increase in Ti-Ni-Zr-Mo in all bio-composites. These findings suggest that HA/BioMEA bio-composites have the potential to be developed as advanced biomaterials with moderate mechanical and biological properties for load-bearing implant applications.
AtıfScopus2WoS1OpenAlex3İncele - MakaleYalnız künye2024Scopus SJRQ2Plant extract-based biosynthesis of silver nanoparticle and silver–zinc nanocomposites-doped hydroxyapatite and its antimicrobial activity
Unal, Ilkay; Aydoğdu, Burcu; Aytar, Mehmet
Hydroxyapatite (HAp) is an essential material in the biomedical field because of its chemical composition, similar to the apatites found in bones. The lack of bactericidal properties of HAp-based materials cannot prevent the adhesion and growth of bacteria. However, it can develop composite biomaterials using nanoparticles (NPs) such as silver (Ag) and zinc (Zn), which exhibit biocidal behaviours to control resistant microorganisms. This study aimed to prepareHAp–AgNPs and HAp–Ag@ZnNPs nanocomposite and evaluate their antimicrobial properties against Gram-positive and Gram-negative bacteria. HAp powders were produced from sheep bone. An aqueous extract of Marrubium astracanicum was used as a reducing and stabilising agent for the synthesis of NPs. The composites were characterized by XRD, SEM–EDX, SEM and FTIR. In vitro biocompatibility assessment was determined by agar well diffusion tests. The HAp–Ag@ZnNPs nanocomposites showed stronger antimicrobial activity than HAp–AgNPs against bacteria and fungi, while pure HAp did not show any effect.
AtıfScopus6WoS5OpenAlex4İncele - MakaleAçık Erişim2023Scopus SJRQ3Morpho-structural and compressive mechanical properties of graphene oxide reinforced hydroxyapatite scaffolds for bone tissue applications
Fidan, Ferzan; Aslan, Naim; Koç, Mümin Mehmet
Hydroxyapatite (HA) is a unique material that has the potential to be used to replace bones and teeth in the field of orthopedics and dentistry since HA exhibits quite similar biological and chemical characteristics to human bone. Hydroxyapatite ceramics are bioactive materials used to repair damaged human tissue. The pores in the porous hydroxyapatite ceramics provide a mechanical interlock, enabling a solid bond and fixation between the implant and bone. In this study, 0.5wt%, 1wt%, and 1.5wt% graphene oxide (GO) reinforced porous HA structures were obtained using the space-holder method to increase the strength of hydroxyapatite with low mechanical strength. NaCl was used as a spacer, and PEG 400 as a binder. Scaffold structures with 40% porosity rates were sintered at 1000 °C under vacuum. Finally, a compression test was applied to the samples which were previously analyzed by SEM, EDS and XRD. The compressive strengths of 0.5%, 1%, and 1.5% graphene oxide reinforced porous HA samples were determined between 8.04 and 31.14 MPa. The highest compressive strength was recorded as 31.14 MPa in the 1% GO added sample, and the lowest compressive strength was recorded as 8.04 MPa in the 1.5% GO added sample. In addition, it was understood that the mechanical properties did not increase regularly with the increase of graphene oxide reinforcing.
AtıfScopus4OpenAlex3
İncele - MakaleYalnız künye2022Scopus SJRQ3Boron-incorporated biocomposite coatings on 316L and NiTi alloys: Enhanced structural, antibacterial activity, and cell viability performances
Aslan, N.; Aksakal, B.; Aksoy, M.E.
Boron doped (5 %, 10%, and 15 wt.%) Hydroxyapatite (B-HA) biocomposites were syntesized and coated on 316L SS and NiTi (Ni-45Ti) metallic substrates by using the electrophoretic deposition process (EPD). The morphological and structural characterization of the coatings was executed using scanning electron microscopy (SEM) and X-ray diffraction devices (XRD). Antibacterial tests were conducted using Escherichia coli (E. coli, JM103) and Staphylococcus aureus (S. aureus, ATCC29293) microorganisms. The mitochondrial activity assay (MTT)-[3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide] was used to examine cell viability and cytotoxicity in Saos-2 osteoblast cells. HA and boron peaks, as well as B-TCP and metallic components, were detected in XRD examinations. Porous morphologies were generated on the surface with boron doped B-HA coatings, as revealed by SEM views. Antibacterial activity studies revealed that both metallic coating groups, notably with boron doping, demonstrated antibacterial activity against gram-negative E. coli and gram-positive S. aureus. The antibacterial activity of the 316L group was shown to be better than that of the NiTi group in comparisonal testing. The syntesized boron-doped biocomposite coatings did not have any detrimental effects on living cells, according to cell viability studies. The cell viability rate was found to be greater in NiTi coatings than in 316 SS coatings, and the impact was amplified by the addition of boron.
AtıfScopus6WoS4OpenAlex7İncele - MakaleYalnız künye2022Scopus SJRQ2Silver/selenium/chitosan co-substituted bioceramic coatings of Ni–Ti alloy: Antibacterial efficiency and cell viability
Say, Yakup; Aksakal, Bunyamin; Sinirlioglu, Zeynep A.
The effects of silver (Ag), selenium (Se), and chitosan (Cht) additives on the antibacterial activity and cell viability of NiTi were investigated. Three different hydroxyapatite (HA)-based bioceramic coatings to improve the antibacterial activity and cell viability of NiTi; HA, HA/Ag, and HA/Se–Cht were applied to NiTi substrates by a sol–gel method. The coated samples were characterized by scanning electron microscopy–electron-dispersive spectroscopy and X-ray diffraction and surface hardnesses were measured. The antimicrobial efficiency of the coatings and uncoated surfaces were tested against Escherichia coli-JM 103 and Staphylococcus aureus-ATCC29293. In vitro cell–material interactions using Saos-2 osteoblast cells were characterized by a 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (mitochondrial activity test) assay for cell viability. A homogeneous, crack-free, and porous surface morphology is achieved in coatings. It has been shown that the Se–Cht additives did not have a significant effect on the surface hardness of the HA coating, but the Ag additive increased the hardness. Through in vitro antibacterial activity and cell viability tests, it was shown that Ag additive to bioceramic coatings significantly increased (p <.05) antibacterial properties but caused a decrease in cell viability. However, although Se–Cht additives did not have a significant effect on antibacterial properties (p <.05), it was observed that they increased cell viability.
AtıfScopus8WoS8OpenAlex2İncele - MakaleYalnız künye2021Scopus SJRQ2Effect of graphene reinforcement on hybrid bioceramic coating deposited on the produced porous Ti64 alloys
Aslan, N.; Aksakal, B.
Porous-Ti64 alloys (P-Ti64), produced at various porosities by hot-pressing technique with the help of Mg spacer, were coated by hybrid-Graphene Oxide (rGO) reinforced-hydroxyapatite (HAp), using the sol–gel method. The synthesized rGO powder was used in reinforcing HAp by the Modified Hummers method having 30 µm particle size and nano (nm) scale layer thickness. Hybrid coatings were executed on Ti64 substrates in four different groups as single-HAp, HAp reinforced with 0.5 wt%, 1.0 wt% and 1.5 wt% rGO for three different porosities (41, 52, and 64%) were characterized by FT-IR, Raman, XRD and SEM. The average 21 µm coating film thicknesses were obtained and desirably, the only superficial pores of the substrates were closed by coating material rather than the inner connected open pores. It was also shown that 0.5 wt% and 1.0 wt% rGO reinforcements into HAp prevented crack formation on the Ti64 surfaces, whereas 1.5 wt% rGo reinforcement and single-HAp coatings caused. The highest adhesion strength values were achieved at low porosities (41–52%) and of 0.5–1.0 wt% rGO reinforcements through the adhesion tests.
AtıfScopus14WoS12OpenAlex20İncele - MakaleYalnız künye2021Scopus SJRQ2Boron-Doped Hydroxyapatite Coatings on NiTi Alloys Using the Electrophoretic Deposition Method: Enhanced Corrosion and Adhesion Performances
Aksoy, M.E.; Aksakal, B.; Aslan, N.; Dikici, B.
Metallic implants are functionalized with coatings due to the need to protect against biological corrosion in the body. Hydroxyapatite (HAp) has desirable biocompatibility and structural properties, but poor mechanical properties limit its use as a standalone coating. In this study, boron-doped hydroxyapatite (B-HAp) biocomposites containing 5, 10, and 15% boron by weight were synthesized by the sol-gel method and applied as a coating to NiTi using electrophoretic deposition (EPD). The deposition was carried out for 60, 90, and 120 s, and sintering at 750 °C for 75 minutes under vacuum. The coated substrates were then characterized by XRD, SEM, and FT-IR, and their adhesion strengths and in-vitro corrosion behaviors in simulated body fluid were compared with uncoated samples. The results showed that the microporous powders formed well-bonded structures, which positively affect adhesion strength. The highest adhesion strength (30 MPa) and corrosion resistance were achieved with 15 wt.% B-HAP coating at 120 s deposition time and 76.5 μm coating thickness.
AtıfScopus18WoS16OpenAlex19İncele - MakaleAçık Erişim2020Scopus SJRQ1Enhanced corrosion properties of biological NiTi alloy by hydroxyapatite and bioglass based biocomposite coatings
Say, Y.; Aksakal, B.
Enhanced corrosion resistance is always an obligatory property in biomedical applications. For this purpose, the surfaces of NiTi alloy were duplex coated both by Hydroxyapatite (HA)/Silver (Ag) and BioGlass (BG)/Silver (Ag) using the sol-gel method. The surface morphologies, and corrosion behaviours of the coatings were examined via SEM, EDS, XRD, and mechanically, by means of hardness as well as adhesion and corrosion tests. SEM analyses showed that the homogenous and crack-free structures were obtained in the biocomposite coatings. Spherical-like structures in the coatings were observed and pitting type of corrosion was formed in the biocomposite coated NiTi surfaces. After the corrosion tests, enhanced corrosion resistance was observed in both HA- and BG- based coatings. However, HA-based HA/Ag coatings on NiTi alloys were obtained to have higher adhesion strength as well as higher corrosion resistance compared to the BG-based biocomposite coatings. The findings in the present study can help the design of future implants with higher corrosion resistance.
AtıfScopus38WoS37OpenAlex42İncele - MakaleYalnız künye2019Scopus SJRQ2Silver/Selenium/Chitosan-doped Hydroxyapatite coatings on biological NiTi alloy: In vitro biodegradation analysis
Say, Y.; Aksakal, B.
Abstract: Nitinol (NiTi) substrates were bioceramic coated by single layer Hydroxyapatite (HA), double layer HA/Silver (Ag) and double-layered HA/Selenium (Se)–Chitosan (Cht) substitutions by sol–gel method. Surface morphologies and adhesion strengths of the obtained coatings were characterized by means of SEM, EDX, XRD, and adhesion tests. Crack-free coatings were obtained in single layer-HA (S1), double layer HA/Ag (S2), and double-layered HA/Selenium–Cht (S3) coatings on NiTi alloys executed via the sol–gel method. Degradation behavior was analyzed in via simulated body fluid (SBF) environment by means of weight loss (%) and ion release rates for 1–4 weeks of immersion periods. The degraded coating particles were measured and metallic ions were detected quantitatively by an inductively coupled plasma–mass spectrometer (ICP–MS). The results show that such coatings could minimize and/or prevent the degradation of metallic ions and weight loss (%) from the coated substrates. From the overall results, HA/Ag double layer biocomposite (S2)-coated NiTi substrates revealed the highest adhesion strength and lowest weight loss and degradation. It was also shown in all groups that the Ni ion release from the NiTi substrates was prevented by the coatings. [Figure not available: see fulltext.].
AtıfScopus10WoS9OpenAlex11İncele - MakaleYalnız künye2018Scopus SJRQ3Synthesis and Characterization of Hydroxyapatite/TiO2 Coatings on the β-Type Titanium Alloys with Different Sintering Parameters using Sol-Gel Method
Dikici, B.; Niinomi, M.; Topuz, M.; Say, Y.; Aksakal, B.; Yilmazer, H.; Nakai, M.
In this study, hydroxyapatite (HA) based composite films were successfully syntheses on the β-type Ti29Nb13Ta4.6Zr (TNTZ). The solutionized TNTZ substrates coated with HA and HA/Titania (TiO2) bioactive composite coatings by sol-gel method under various sintering parameters related to sintering temperatures and heating ramp rates. Microstructural observations of the coatings revealed that apatite was formed on the substrates. The hardness values of the coatings increase with increasing both the sintering temperature and the TiO2 concentration in the coatings layer. However, it was found that the heating ramp rate of the sintering was not affecting the hardness values so much. Also, the hardness values of the HA/TiO2 composite coatings at all sintering temperatures were higher than only HA coated TNTZ samples due to the existence TiO2 phases in the HA matrix. Results indicating that the doping of HA with TiO2, improve the physical consistency between the coating layer and the substrates and provide a better inter-particle bonding due to the existence TiO2 phases in the HA.
AtıfScopus42OpenAlex43İncele - MakaleYalnız künye2017Scopus SJRQ1Biodegradation of hydroxyapatite coated Rex-734 alloy with silver and selenium/chitosan substitutions: In vitro analysis
Aksakal, B.; Say, Y.; Buyukpinar, Ç.; Bakirdere, S.
Hydroxyapatite (HA) based bioceramic coatings; such as single-HA, double layered with Silver-Ag, Selenium-Se and Chitosan substitutions on Rex-734 alloy were executed by using the sol-gel method. Surface morphologies and adhesion strengths of the obtained coatings were investigated and coating material weight losses and metal ion releases from the substrates were determined in SBF (Simulated Body Fluid) environment. The coatings were characterized by SEM, EDS, XRD and adhesion strengths between the substrate and bioceramic coatings were measured with adhesion tests. SEM analyses revealed that crack-free surface morphologies were obtained in all bioceramic coatings. The coatings were kept in SBF for immersion periods from one to four weeks and the weight loss (%) in coatings and changes in ion release rates were determined. HA/Ag double layered coatings applied on the Rex-734 alloy increased the adhesion strength and accordingly reduced the weight losses (%) of coating materials in SBF. Se/Chitosan double layered coatings were found to decrease the adhesion strength and increase the weight losses (%) in SBF. Additionally, all bioceramic coatings were observed to prevent the elemental ion release by physical barrier effect for the release of metal ions during the four weeks immersion period in SBF.
AtıfScopus12WoS11OpenAlex12İncele - MakaleYalnız künye2017Scopus SJRQ1The effect of Zirconia/Yttria/Silver substitutions on mechanostructure and cell viability of the synthesized bioceramic bone grafts
Aksakal, Bunyamin; Demirel, Mehtap
Hydroxyapatite (HA) based biografts were synthesized by substitution of Zirconia (Zr), Yttria (Y2O3) and Silver (Ag) using the sol-gel method. Fabricated bone grafts (H40ZrYt and H50Yt10) were compared with a control biograft. The effects of Zr and Y2O3 and Ag additions on the morphological, mechanical and cell viability of the synthesized biografts were analyzed. The biografts were characterized by X-ray Diffractometer (XRD) and Scanning Electron Microscope (SEM). All biografts were then embedded into the drilled holes (D=3.2 mm) in rabbit femurs. The rabbits were then sacrificed after twelve weeks. Three-point bending (3-PB) tests were conducted on defected and grafted regions. Flexural strength values were found to be 347, 149 and 180 MPa, for the H40ZrYt, H50Yt10 and the control/commercial graft, respectively. Cell viability results indicated that the percentage viability ratios slightly increased after the substitution of Ag into the H50Yt10 biograft at 0.1 and 0.3 µg/ml concentrations and into the H40ZrYt biograft at a 0.1 µg/ml concentration. Although the cell viability was a bit lower in the H50Yt10 graft, the H40ZrYt graft achieved better results compared to the counterpart grafts. Furthermore, the hardness of both of the novel fabricated grafts were found to be higher than the control/commercial graft, however, as the flexture strength of H40ZrYt was higher but H50Yt10 was lower than the control/commercial graft.
AtıfScopus11WoS10OpenAlex13İncele - MakaleYalnız künye2016Scopus SJRQ3Optimization of Cadmium Removal from Water by Hydroxyapatite Using Experimental Design Methodology
Ince, Olcay Kaplan; Ince, Muharrem; Karaaslan, Nagihan M.; Yonten, Vahap
The presence of cadmium in water is a serious threat to the environment. The removal of cadmium using hydroxyapatite as an adsorbent was studied in an aqueous system. Hydroxyapatite was prepared to process the adsorption of cadmium from aqueous solution. Experimental design methodology and response surface methodology (RSM) with a quadratic model associated with central composite design was used to optimize the pH, initial heavy metal concentration, final volume, and adsorbent dosage for the removal of cadmium. Analysis of variance identified significant factors on each parameter. RSM indicated that a pH of 8.5, a sample volume of 166 mL, an adsorbent of dosage 0.57 g, and a contact time of 82 min were optimal for the adsorption of Cd(II). Under these conditions, the removal of Cd(II) was 895 mg g(-1).
AtıfWoS17OpenAlex15İncele - MakaleYalnız künye2016Scopus SJRQ1Effect of hydroxyapatite/SiO2 hybride coatings on surface morphology and corrosion resistance of REX-734 alloy
Say, Yakup; Aksakal, Bunyamin; Dikici, Burak
REX-734 stainless steel alloy was coated with hydroxyapatite (HA)-silicon dioxide (SiO2) composite (hybride) coatings by using the sol-gel method. Surface morphologies, adhesion resistances and corrosion behaviors of the coatings were examined and the characterization of the coatings was performed by using XRD, SEM, and EDS. It was observed that porous and crack-free surface morphology enhanced adhesion strength of the coatings. Through the shear tests, it was found that the adhesion resistance was 25.14 MPa in HA coatings and 25.47 MPa in HA-SiO2 coatings. Corrosion analyses of the coatings were performed by using potentiodynamic polarization (PDS) tests. It was determined that corrosion dimples formed on the coating surface and the corrosion resistance in HA+SiO2 coatings increased with decreasing porosity; however, in the further steps of corrosion, it reached to the base material by causing a pitting effect on the coated surface. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
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